Tags · Status
data table
Contains a real tabulated dataset.
Related in this group: solved · open question · needs a source · long read · beginner friendly · worked example · disputed
117 topics · page 1 of 4
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Cleaning a self-reported dataset and what you throw away — what changed since
Posting this under the heading it deserves: Cleaning a self-reported dataset and what you throw away — what changed since Everything below is what sits behind that. What changes if the standard account of…
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2 | 2k | 1h | |
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What a reversed-phase purity number actually is
The question in the title: What a reversed-phase purity number actually is I will give what I have already checked below so nobody repeats it. I would like to understand what this number means before I repeat…
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+87 | 101 | 27k | 4h |
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Named, unnamed and unspecified impurities as regulatory categories — the long version
Named, unnamed and unspecified impurities as regulatory categories — the long version — setting out what I have, and where I think it stops being reliable. Two reports on the same lot, and I would like help…
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+112 | 120 | 7.6k | 5h |
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Follow-up: Comparing two chromatograms from different laboratories, properly
Comparing two chromatograms from different laboratories, properly — setting out what I have, and where I think it stops being reliable. I would like to understand what this number means before I repeat it…
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+62 | 67 | 12k | 9h |
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A 40-week log with the measurement method stated — what changed since
A 40-week log with the measurement method stated — what changed since Writing it up because I had to work it out twice and would rather nobody else did. Posting a small dataset on 40-week log. It is mine, it…
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+9 | 13 | 2.1k | 9h |
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Deletion sequences: expected mass shifts by residue — the long version
On the subject in the title: Deletion sequences: expected mass shifts by residue — the long version Working notes rather than a conclusion. Deletion sequences keeps being re-asked here and I think that is…
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+21 | 25 | 6.9k | 10h |
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Endotoxin and why it is a separate question from purity — what changed since
On the subject in the title: Endotoxin and why it is a separate question from purity — what changed since Working notes rather than a conclusion. What changes if the standard account of Endotoxin is wrong? I…
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+78 | 91 | 1k | 10h |
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Seven-day rolling means and why weekly readings mislead
Seven-day rolling means and why weekly readings mislead Writing it up because I had to work it out twice and would rather nobody else did. Posting a series rather than a conclusion, with the method first.…
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+109 | 125 | 42k | 10h |
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Why 99.2% and 97.8% on the same lot can both be correct
Why 99.2% and 97.8% on the same lot can both be correct I have a specific reason for asking rather than idle curiosity, and the context is below. I would like to understand what this number means before I…
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+16 | 20 | 3.1k | 11h |
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Comparing my trajectory with the trial curves, carefully — a second dataset
Comparing my trajectory with the trial curves, carefully — a second dataset — setting out what I have, and where I think it stops being reliable. Maintenance rather than loss, which is the part of this that…
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+77 | 81 | 16k | 11h |
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Why the cheapest option is often not the cheapest
Why the cheapest option is often not the cheapest I have a specific reason for asking rather than idle curiosity, and the context is below. Cheapest option: setting out the arithmetic in full, because I have…
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+19 | 23 | 1.2k | 12h |
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An 18-month record including the parts that went badly
An 18-month record including the parts that went badly — setting out what I have, and where I think it stops being reliable. Asking about 18-month record on behalf of the question I keep seeing asked badly,…
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+77 | 81 | 17k | 12h |
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Shoulders, tangent skims, and defensible integration
Posting this under the heading it deserves: Shoulders, tangent skims, and defensible integration Everything below is what sits behind that. Setting out an integration problem with the actual figures, because…
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+16 | 20 | 11k | 13h |
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A community side-effect dataset, with its response rate and biases
A community side-effect dataset, with its response rate and biases — setting out what I have, and where I think it stops being reliable. Community side-effect dataset: setting out the arithmetic in full,…
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2 | 5.1k | 19h | |
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Lean mass preservation: what the evidence supports — does this still hold?
Asking directly, because I could not find a straight answer: Lean mass preservation: what the evidence supports — does this still hold? What changes if the standard account of Lean mass preservation is wrong?…
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+112 | 122 | 5.2k | 20h |
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[2026 update] Waist circumference technique and its repeatability
Posting this under the heading it deserves: Waist circumference technique and its repeatability Everything below is what sits behind that. An honest uncertainty about Waist circumference technique rather than…
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+23 | 27 | 5.9k | 21h |
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Blinding yourself: practical methods and their limits — the long version
Blinding yourself: practical methods and their limits — the long version Writing it up because I had to work it out twice and would rather nobody else did. A narrow question about Blinding yourself,…
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+7 | 11 | 1.8k | 22h |
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[2026 update] Comparing prices across jurisdictions without misleading yourself
On the subject in the title: Comparing prices across jurisdictions without misleading yourself Working notes rather than a conclusion. Comparing prices across jurisdictions keeps being re-asked here and I…
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2 | 809 | 23h | |
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Cleaning a self-reported dataset and what you throw away
Cleaning a self-reported dataset and what you throw away — setting out what I have, and where I think it stops being reliable. Collecting what is known about cleaning a self-reported dataset in one place,…
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2 | 28k | 1d | |
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Washout with a one-week half-life: the arithmetic — does this still hold?
Washout with a one-week half-life: the arithmetic — does this still hold? — that is the question, and I have not found it answered plainly anywhere I have looked. Washout: setting out the arithmetic in full,…
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+41 | 45 | 12k | 1d |
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Revisiting: Theoretical plates: useful number or ritual?
Asking directly, because I could not find a straight answer: Revisiting: Theoretical plates: useful number or ritual? Asking about Theoretical plates directly, because I have read four threads on it and each…
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+16 | 21 | 1.2k | 1d |
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Impurity thresholds: where the common numbers come from
Impurity thresholds: where the common numbers come from — setting out what I have, and where I think it stops being reliable. I have spent a fortnight trying to pin impurity thresholds down and I want to set…
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+11 | 15 | 825 | 2d |
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Coming back to: A community side-effect dataset, with its response rate and biases
Posting this under the heading it deserves: A community side-effect dataset, with its response rate and biases Everything below is what sits behind that. Community side-effect dataset — I have the observation…
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+96 | 101 | 33k | 2d |
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Designing a personal experiment that could change your mind — one year on
Designing a personal experiment that could change your mind — one year on — setting out what I have, and where I think it stops being reliable. Two things I would like separated before anyone answers on…
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+74 | 80 | 17k | 2d |
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[2026 update] Why 99.2% and 97.8% on the same lot can both be correct
Why 99.2% and 97.8% on the same lot can both be correct — that is the question, and I have not found it answered plainly anywhere I have looked. I would like to understand what this number means before I…
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+1 | 5 | 719 | 2d |
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Ultrasound and skinfolds: operator dependence in practice
Ultrasound and skinfolds: operator dependence in practice — setting out what I have, and where I think it stops being reliable. Trying to establish the boundary conditions on ultrasound and skinfolds. The…
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+72 | 76 | 2.7k | 2d |
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Blinding yourself: practical methods and their limits
On the subject in the title: Blinding yourself: practical methods and their limits Working notes rather than a conclusion. A methods question rather than a substantive one, about blinding yourself. Everyone…
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+40 | 44 | 33k | 5d |
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Manufacturer assistance programmes and their eligibility rules
On the subject in the title: Manufacturer assistance programmes and their eligibility rules Working notes rather than a conclusion. I have spent a fortnight trying to pin manufacturer assistance programmes…
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+37 | 42 | 32k | 11d |
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[2026 update] Area percent versus weight percent: the confusion that causes most arguments
On the subject in the title: Area percent versus weight percent: the confusion that causes most arguments Working notes rather than a conclusion. Proposing that Area percent versus weight percent deserves a…
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+65 | 70 | 1.1k | 16d |
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Carryover and the ghost peak from last week's standard — what changed since
Carryover and the ghost peak from last week's standard — what changed since Writing it up because I had to work it out twice and would rather nobody else did. What changes if the standard account of Carryover…
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+98 | 114 | 37k | 22d |